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Smart Image Examples Embodiment 1 [0031] Add N-protected-L-histidine (6.20g, 0.01mol) in the reaction flask, thionyl chloride (9.52g, 0.08mmol) and heat to reflux, add DMF (30mL), control temperature and reflux, reduce The unisolated intermediate III (according to 100% yield) was distilled under high pressure with solvent

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